Analytical Techniques

  • X-ray powder and single crystal diffraction (XRD)
  • Neutron time-of-flight powder diffraction (NPD)
  • X-ray powder total scattering and pair distrobution function analysis (PDF)
  • X-ray reflectometry (XRR)
  • X-ray fluorescence (XRF)
  • Total reflection X-ray fluorescence (TXRF)
  • Electron probe microanalysis (EPMA)
  • Scanning electron microscopy (SEM)
  • Energy-dispersive X-ray spectroscopy (EDS)
  • Thermogravimetric analysis (TGA)
  • Differential scanning calorimetry (DSC)
  • Inductivley coupled plasma optical emission spectroscopy (ICP-OES)
  • UV/VIS/IR diffuse reflectance

Instrumentation

  • Parr Autoclaves
  • Hydrothermal cold-seal vessels
  • Tube furnaces
  • Deltech box furnaces
  • Gas-mixing furnaces
  • Piston-cylinder pressure apparatus
  • Paris-Edinburgh pressure apparatus
  • Multi-anvil high pressure apparatus
  • Ultrasonic and aerodynamic levitation
  • Welding and lathe machining
  • 3D printing

Professional Development

  • Total Reflection X-Ray fluorescence TXRF Analysis - ICDD Semiconductor Wafer Analysis Course, EAG Laboratories, October 2016
  • Semiconductor Device Manufacturing Overview - AVS Short Course, EAG Laboratories, June 2016
  • Evolutionary Structure Prediction Using the USPEX Code workshop, Stony Brook University, 2012.
  • Advanced Simulation Techniques for Total Scattering Data workshop, Santa Fe, NM, 2012.
  • Nanoscale Ordered Materials Diffractometer workshop, Oak Ridge National Laboratory, 2011.
  • DISCUS workshop, Stony Brook University, 2011.
  • National School on Neutron and X-ray Scattering, Argonne & Oak Ridge National Labs, 2010.
  • Communicating Science Workshop with Alan Alda, Stony Brook University 2009.

DOE National Laboratory Facilities Experience

Argonne National Laboratory (ANL) Argonne, IL, Advance Photon Source

  • 11-BM – high-resolution powder X-ray diffraction
  • 11-ID-B – high-energy total X-ray scattering and atomic pair distribution function
  • 11-ID-C – in situ high-energy total X-ray scattering on levitated liquids
  • 13-BM-D – in situ high-pressure X-ray diffraction

Oak Ridge National Laboratories (ORNL) Oak Ridge, TN, Spallation Neutron Source

  • POWGEN – powder neutron scattering
  • NOMAD – neutron total scatting and atomic pair distribution function
  • SNAP – in situ high pressure powder neutron scattering

Brookhaven National Laboratory (BNL) Upton, NY, National Synchrotron Light Source

  • X17B2 – in situ high pressure X-ray energy dispersive diffraction
  • X17B3 – in situ diamond anvil cell high energy total X-ray scattering
  • X17A – high-energy total X-ray scattering and atomic pair distribution function
  • X26A – X-ray microprobe
  • X16C – high-resolution powder X-ray diffraction

Crystallographic Software

     GSAS / EXPGUI           TOPAS
     Fit2d                             PDFgetX2
     PDFGui                         DISCUS
     WinGX                          SHELX
     CrystalMaker                Jade